Preservation Methods For Pure Cultures

Preservation is a process of maintaining pure culture for extended periods in a viable condition without any genetic changes. Once a pure culture has been obtained from the mixture, the microbes may be maintained in the laboratory over long periods. The most important factor of preservation is to stop microbial growth or at least suppress the growth rate.


Objectives of Preservation:


• To maintain isolated pure cultures for longer periods in viable conditions.

• To avoid contamination.

• To restrict genetic changes.


Several techniques are used to preserve cultures viz. period transfer in fresh medium or Subculturing, Storage in sterile soil, Saline suspension, Refrigeration, Paraffin Method, Cryopreservation, and Lyophilization.


1. Subculturing: Strains are maintained by periodically preparing a fresh culture from the previous stock culture. Culture medium, storage temperature and the time interval at which transfers are made vary with the species. Nutrient agar medium is commonly used where most of the heterotrophs remain viable for several months.


2. Storage in sterile soil: The soil is prepared by mixing enough sand with rich garden soil that makes it friable and easy to handle. A small amount of calcium carbonate may be added and the mixture is transferred to screw-capped tubes or tubes plugged with cotton. The tubes are autoclaved until complete sterility. This soil is widely used in preservation cultures that form "spores". A thick suspension of spores is added to the sterile soil to this. Moisture is removed by placing the cap and maintaining reduced pressure over a drying agent.


3. Saline suspension: Sodium chloride in high concentration is frequently an inhibitor of bacterial growth. Bacteria are suspended in a 1% salt solution. The tubes are stored at room temperature. Whenever needed the transfer is made on an agar slant.


4. Refrigeration: Pure cultures are also stored at 0-4°C either in refrigerators or in cold rooms. This method is applied for a short duration (2-3 weeks for bacteria and 3-4 months for fungi) because the metabolic activities of the microorganisms are greatly slowed down but not stopped.


5. Paraffin method: This is a simple and economical method of maintaining pure cultures of bacteria and fungi. In this method, sterile liquid paraffin is poured over the slant (slope) of the culture and stored above at room temperature. The layer of paraffin ensures anaerobic conditions and prevents dehydration of the medium. This condition helps microorganisms or pure culture to remain in a dormant state. Hence, the culture is preserved for several years. This method is also known as Agar Slant Culture Covered with Oil.


6. Cryopreservation: Cryopreservation (i.e., freezing in liquid nitrogen at −196°C) helps in the survival of pure cultures for long storage times. In this method, the microorganisms of the culture are rapidly frozen in liquid nitrogen at −196°C in the presence of stabilizing agents (glycerol). It prevents the formation of ice crystals and promotes cell survival.


7. Lyophilization: It is also known as Freeze-Drying. It is the method of removal of the frozen solvent by sublimation under vacuum and unfrozen solvent by desorption. In this method, the culture is rapidly frozen at a very low temperature (−70°C) and then dehydrated by vacuum. Under these conditions, the microbial cells are dehydrated and their metabolic activities are stopped; as a result, the microbes go into a dormant state and retain viability for years. Lyophilized or freeze-dried pure cultures and then sealed and stored in the dark at 4°C in refrigerators.


Cultivation of Anaerobes:


Anaerobic microorganisms are widely spread in the environment. They do not require oxygen for their growth. Sometimes these organisms are very toxic. There are two types of anaerobes namely, facultative anaerobes, obligate anaerobes, and aerotolerant anaerobes.


• Facultative anaerobes: They are organisms that can grow in the presence or absence of oxygen. They obtain energy by both respiration as well as fermentation. Some examples of facultative anaerobic bacteria are Staphylococcus spp. Streptococcus spp., Escherichia coli, Salmonella, Listeria spp. and Shewanella oneidensis.


• Obligate anaerobes: They are organisms that can grow totally in the absence of oxygen. Oxygen is toxic for their normal growth. Examples: Actinomyces, Bacteroides, Clostridium, Fusobacterium, Peptostreptococcus, Porphyromonas, Prevotella, Propionibacterium, Veillonella, etc.


• Aerotolerant anaerobes: They are organisms that cannot use oxygen for growth but are able to tolerate its presence. They have superoxide dismutase and peroxidase but do not have catalase. Examples: Streptococcus, Clostridium, and Actinomyces.


Principle: Reduce the O2 content of the culture medium and remove any oxygen already present inside the system or in the medium. Oxygen is ubiquitous in the air so special methods are used to culture anaerobes. Four types of culture media are used likely:


1. Special Anaerobic Culture Media

2. Anaerobic Chamber

3. Anaerobic Bags or Pouches

4. Anaerobic Jars.


1. Special Anaerobic Culture Media: This media is also known as pre-reduced media. During preparation of this media, the liquid culture medium is boiled by holding in a boiling water bath for 10 minutes to remove the dissolved oxygen. Liquid media soon become aerobic so to keep media anaerobic, reducing agents such as cysteine 0.1%, ascorbic acid 0.1%, and sodium thioglycollate 0.1% are added to lower the oxygen content.


Oxygen-free N2 is bubbled through the medium to maintain anaerobic conditions. The medium is then dispensed into tightly stoppered tubes and autoclaved for sterilization. Such tubes are stored for many months before being used. During inoculation, the tubes are continuously flushed with oxygen-free CO2 with a gas cannula, re-stoppered, and incubated (Fig).

Pre-reduced culture media

Fig: Pre-reduced culture media


The inoculum of the bacterium is inserted deep in the medium in contact with the meat. Meat particles are placed in 30 ml bottles to a depth of about 2.5 cm and covered with about 15 ml broth.


Cooked meat broth is suitable for growing anaerobic bacteria in air and also for the preservation of their stock cultures which is also known as ‘Robertson’s bullock-heart medium’. Thioglycollate broth is also a useful medium for anaerobes. Some other media such as Brucella blood agar, Bacteroides, bile, aesculin agar, phenyl ethyl alcohol agar, kanamycin blood agar, etc. are used for recovering anaerobes. Vitamin K, haemin, and yeast extract are used as essential nutrition for all the anaerobes media.


2. Anaerobic Chamber: An Anaerobic chamber is an ideal anaerobic incubation system, which provides an anaerobic environment for the inoculation of media and the incubation of cultures. The chamber is made up of a plastic anaerobic glove box that contains an atmosphere of H2, CO2, and N2. Glove ports and rubber gloves are used during experimentation to perform manipulations within the chamber. There is an air-lock with inner and outer doors. Culture media are placed within the air-lock with the inner door. The air of the chamber is removed by a vacuum pump connection and replaced with N2 through the outer doors. The culture media are then transferred from the air-lock to the main chamber containing H2, CO2, and N2. A circulator fitted in the main chamber circulates the gas atmosphere through pellets of palladium catalyst causing any residual O2 present in the culture media to be used up by reaction with H2. The existence function of CO2 in the chamber is because of many anaerobic bacteria for their optimum growth. Hence, when the culture media becomes completely anaerobic, they are inoculated with bacterial culture and are placed in an incubator in the chamber (Fig).

Anaerobic chamber Vacuum pump connection

Fig: Anaerobic chamber Vacuum pump connection


3. Anaerobic Bags or Pouches: Anaerobic bags or pouches make convenient containers when only a few samples are to be incubated anaerobically. They are available commercially. Bags or pouches have an oxygen removal system consisting of a catalyst and calcium carbonate to produce a CO2-rich atmosphere. One or two inoculated plates are placed into the bag and the oxygen removal system is activated and the bag is sealed and incubated. Plates are examined for growth without removing the plates from the bag. These bags are also useful in the transport of biopsy specimens for anaerobic cultures.


4. Anaerobic Jars (or GasPak Anaerobic System):


Anaerobic Jar

Fig: Anaerobic Jar


These anaerobic jars are required for obtaining surface growth of anaerobic bacteria in anaerobic conditions. The most reliable and widely used anaerobic jar is the Melntosh-Fildes’ anaerobic jar. It is a cylindrical vessel made of glass or metal with a metal lid, which is fitted by a clamp. The lid possesses two tubes with taps, one acting as a gas inlet and the other as an outlet. On its under-surface, it carries a gauze sachet carrying palladium pellets, which acts as a room-temperature catalyst for the conversion of hydrogen and oxygen into water. Palladium pellets act as catalysts (Fig).


Inoculated culture plates are placed inside the jar and the lid is clamped tightly. The outlet tube is connected to a vacuum pump and the air inside is evacuated. The outlet tap is then closed and the gas inlet tube is connected to a hydrogen supply from where hydrogen is drawn rapidly. After 5 minutes inlet tube is further opened and the catalyst creates a reduced pressure within the jar due to the conversion of hydrogen and leftover oxygen into water. The jar is left connected to the hydrogen supply for about 5 minutes and then the inlet tube is closed and the jar is placed in the incubator.


The gasPak is now the method of choice for preparing an anaerobic jar. The gasPak is commercially available as a disposable envelope containing chemicals that generate hydrogen and carbon dioxide when water is added. After the inoculated plates are kept in the jar, the gasPak envelope with water is added and is placed inside and the lid screwed tight. The culture plates should be removed from the jar and placed in the oxygen-free holding system. From there culture plates should be removed one by one for rapid microscopic examination of colonies, and then quickly returned to the holding system.

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